https://www.journals.elsevier.com/journal-of-materials-research-and-technology Availableonlineatwww.sciencedirect.com
Original
Article
Mechanical
and
durability
properties
of
ground
calcium
carbonate-added
roller-compacted
concrete
for
pavement
Sadik
Alper
Yildizel
a,
Gokhan
Calis
a,∗,
Bassam
A.
Tayeh
baKaramanogluMehmetbeyUniversity,FacultyofEngineering,CivilEngineeringDepartment,Turkey bCivilEngineeringDepartment,FacultyofEngineering,IslamicUniversityofGaza,Palestine
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Articlehistory: Received25June2020 Accepted14September2020 Availableonline30September2020
Keywords:
Roller-compactedconcrete Groundcalciumcarbonate Freeze–thawcycles
Magnesiumsulphateresistance Durabilityproperties
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This research aimed toinvestigate the mechanical and durability properties of roller-compacted concrete (RCC) containing ground calcium carbonate (GCC). Five different mixturecombinationswerepreparedbyreplacingcementwithGCCatthelevelsof5%, 10%,15%,20%and25%byweight.Thewatercontentsofthemixturewereoptimisedwith themaximumdensitymethod.ThecompressiveandflexuralstrengthsoftheRCCmixtures wereevaluatedupto90days.Durabilitycharacteristics,suchaswaterabsorptionrates, sul-phateandfreeze–thawresistances,werealsoevaluatedinthisstudy.TheGCCinclusionof upto15%increasedthemechanicalstrengthvaluesandenhancedthedurability charac-teristicsoftheRCCmixtures.Scanningelectronmicroscopyimagesoftheadditional15% GCCwerealsoutilised.ResultsrevealedthatGCCinclusionexhibitedanimprovementin thedurabilitypropertiesofthespecimens.
©2020TheAuthor(s).PublishedbyElsevierB.V.Thisisanopenaccessarticleunderthe CCBY-NC-NDlicense(http://creativecommons.org/licenses/by-nc-nd/4.0/).
1.
Introduction
Roller-compactedconcrete(RCC)hasbeenwidelystudieddue toitsbenefits,suchaslowapplicationcost,high-density con-structiontechnologyandreducedcementcontents,compared with other types of concrete pavement [1]. RCC is gener-allydesignedwithzero-slumpvaluesandcompactedsimilar to soil [2,3]. Moreover, considerable amounts of construc-tioncompactionenergyandincreasedaggregatecontentsare requiredforthetraditionalRCCdesigns[4].
RCC structures are continuously and directly exposed toenvironmentaldeteriorativefactors,suchasfreeze–thaw cyclesand chemicals.Therefore, inadditiontoits strength
∗ Correspondingauthor.
E-mail:gokhancalis@kmu.edu.tr(G.Calis).
characteristics,thedurabilitypropertiesofRCCpavementsare alsovital[5].Especiallyincoldregions,deteriorationsonRCC structuresareacceleratedwithcontinuousfreeze–thawcycles andtheuseofde-icingsalts[6].Concretedamages,suchas cracksandsurfacescaling,canemergeasaresultof harm-fulmechanisms.Numerousstudieshavebeenconductedto predict andeliminatetheeffectsoffreeze–thawcycles and chemicalattacks[7,8].Theoptimisationofwater-to-cement ratio and the usage ofsupplementary cementitious mate-rials andair-entrainingchemicalswerewidelyevaluatedin manydurabilityreports[9–11].Inaddition,air-entrainedRCC productionispopularamongstscientistsinthelastdecade; however, itsapplicationwaslimitedduetoutilisation diffi-cultiesofair-entrainingchemicalsduringtheRCCdesign[8].
The interest in utilising supplementary cement materi-als to formulate nature-friendly and economical concrete has increased in recent years due to environmental rea-https://doi.org/10.1016/j.jmrt.2020.09.070
2238-7854/©2020The Author(s).Published byElsevier B.V.Thisis anopen accessarticleunderthe CC BY-NC-NDlicense (http:// creativecommons.org/licenses/by-nc-nd/4.0/).
sons.Therefore,manystudieshavebeenfocusedoncement replacementand alternative binding materialsin the con-crete productionindustry [12–14]. Utilising ground calcium carbonate (GCC)as acementreplacementmaterialin con-crete mixturesmay improve its strength and cohesiveness behaviour.GCCisgenerallyusedtoeliminatestructuralpores inthemicrostructureofconcretes.Inaddition,GCCusagein theRCCdesigncanlimitthenegativeeffectofbleedingand shrinkagemechanisms[15].
Themechanical and durabilitypropertiesofGCC-added RCCwereinvestigatedinthisstudy.Themechanical exper-imental study focused on the compressive and flexural strength test results at 7, 28 and 90 days. Durability tests include determination of sulphate and freeze–thaw resis-tancesandwaterabsorptiontests.Inaddition,theabrasion resistanceofthepreparedmixeswasmeasured with sand-blasting.
Supplementary cementitious materials, suchas flyash, silica fume and furnace slags, can be used as partial replacements of cement in concrete mixture designs to reducecement production-originatedcarbon dioxide emis-sions[16,17]. The addition ofthese kinds ofmaterials not onlylimitsthenegativeimpactsontheenvironmentbutalso resultsinenhancedlong-termmechanicalbehavioursof con-cretes.Supplementarycementitiousmaterialshavealsobeen widelyusedinvarioustypesofconcretes,includingRCC pave-ments[18,19].Severaltypesofresearchhavebeenfocusedon thereplacementofcementbynaturalandindustrialmaterials [18,20].Literaturereportsindicatedthatcementreplacement materialscanbeusedtoenhancethemechanicaland dura-bilitypropertiesoftheRCCpavements.
RCCisespeciallypreferredforroadanddamconstruction projectsduetoits rapidsettingcharacteristics.Inaddition, RCC ismoresuitable forthe construction ofroad surfaces comparedwiththeasphalticcoversbecauseitdevelopshigh compressivestrengths[21,22].TheuseofRCCindamprojects requireshighwater-to-cementratiosandlowcement quanti-ties.Lowwater-to-cementcontentusageinRCCroadsleads to decrease in bleeding [23]. The bleeding and shrinkage behavioursoftheconcretecanalsobelimitedbyGCC inclu-sion. GCCadditions increased the compressive strength of
theconcretewiththecuringageaccordingtotherelated lit-erature studies[24–26]. Theprincipal advantageofutilising GCCinconcretemixesnotonlyleadstoimprovedmechanical anddurabilitypropertiesbutalsoprovideslessCO2emissions
caused bythecement industry.However,high dosageGCC additionascementreplacementmaterialsinconcretemixes canresultindecreasedstrengthvalues[27].Thereactivityof GCCisrelatedtoitsspecificsurfacearea,andsmallparticles haveanadditionalsurfaceareaforC3Areactions[25].
Grind-ingoftheGCCrequireslesserenergyconsumptioncompared withthatofothercementreplacementmaterialsbecauseGCC haslowhardness[28].
TheGCCinclusiontoconventionalconcretehasprovided improved structural, mechanical and durability properties accordingtoliteraturereportsinthelastdecades.However, resultsontheGCCadditiontoRCCmixturesarelimited.This study aimsto enrich the available experimentaldata con-cerning GCC utilisationinRCC pavementstoreach aclear understandingofitsbehaviour.
2.
Materials
and
methods
2.1. Materialsandmixturepreparations
River sand was utilised asfine aggregates, and crush rock materialcontaininglimestonewasusedascoarseaggregates inthisexperimentalwork.Themaximumaggregatesizewas chosenas20mmtopreventsegregation.Allaggregateswere cleanedfromanyorganicmaterialsfollowingtheair-drying process. Theaggregates were utilisedaccording tothe ACI requirements [29]. A commercial product, Betocarb®, was usedastheGCCfillermaterial.Thecombinedgradationcurves and material propertiesofthe aggregates are presentedin Fig.1andTable1,respectively.Scanningelectronmicroscopy (SEM)imagesoftheGCCparticlesareprovidedinFig.2.
CemItypecementconformingtotheEN197[32]standard wasutilisedasthethebindermaterial.Table2presentsthe chemicalandphysicalpropertiesofthecementandGCC.
Table3showsthemixtureproportionsofthestudiedRCC. SixdifferentRCCmixtureswerepreparedinthis
Table1–Aggregatematerialproperties.
MaterialProperty FineAggregate(FA) CoarseAggregate(CA) Betocarb®
ModulusofFineness 2.62 –
SpecificGravity 2.64 2.76
Bulking,% 7.3 –
SiltContent,% 0.72 –
Waterabsorption(ASTMC138)[30],% 1.1 3.2
LosAngelesabrasion(ASTMC131)[31],% 21 24
TotalMoisture,% 0.10 0.40
Bluevalue,g/kg <10
d50%,(m) 5–30
Table2–Materialpropertiesofthecement.
Chemicalandphysicalproperty Cement GCC(Betocarb)
Iron(III)oxide(Fe2O3) 3.52 0.052
Calciumoxide(CaO) 60.24 97.81
Aluminiumoxide(Al2O3) 4.39 0.055
Magnesiumoxide(MgO) 2.39 1.89
SiO2 – 0.119
SrO – 0.024
Sulphurtrioxide(SO3) 2.64 0.019
K2O – 0.015
Freecalciumoxide(CaO) 1.73 –
LOI,% 2.92 –
Morphology – Cubicorhexagonal
Colour – White
Specificgravity 3.11
Soundness,mm 0.51 –
Fineness,cm2/g 3620 –
Settingtime,min.(Ini.–Fin.) 175–225 –
Compressivestrength,MPa(2,7and28days) 27.90,42.85,52.14 –
Table3–RCCmixtureproportions.
Mixturecode Cement(kg) GCC(kg) FA(kg) PA(kg) W/(C+GCC) Compactionratio(%) Optimumwatercontent(%)
R 260 0 750 1128 0,4 100 5.29 RCC-5 247 13 750 1128 0,41 100 5.34 RCC-10 234 26 750 1128 0,42 100 5.42 RCC-15 221 39 750 1128 0,44 100 5.50 RCC-20 208 52 750 1128 0,45 99 5.55 RCC-25 195 65 750 1128 0,46 98 5.6
Fig.2–SEMimagesofGCCparticles.
tal study,and thesemixtures were coded in linewith the GCCinclusions.‘R’definesthereferencemixturewithnoGCC content.Othermixtureswereclassifiedas‘RCC-x’,where‘x’ representsthecementreplacementratioofGCCbyweight.
ThecementreplacementlevelswithGCCwereconsidered tobe5%,10%,15%,20%and25%byweight.Thespecimens werecompactedinthreelayerswithacompactorattheblow countof1000and1870r/min(10kgsurcharge)inaccordance withthe ASTM C1435procedure [33].Theoptimumwater content oftheconcretes isprovidedinTable 3. Cylindrical specimens(150mm×300mm)withwater-to-cementratiosof 0.35,0.4,0.45and0.50werepreparedtodeterminethe opti-mummoisturecontentoftheRCCmixtures. Theoptimum watercontentoftheRCCmixesgenerallyvariesbetween4.6% and5.6%[34].AllthepreparedRCCspecimenwatercontents werewithinthelimitsoftheserates.
Themixtureswere preparedwitha60Lpan mixer.The aggregates,namely,Betocarb® andcement,wereinitiallydry mixed,andthentherequiredwaterwasadded.Themixerrate waskeptconstantat250r/minfor5mintoobtaina homoge-nousmixture. Thespecimenswere cured atthe laboratory temperaturefor24h.Then,allspecimenswereremovedfrom themouldsandkeptunderlime-saturatedwater(23◦C)until
themechanical tests.Theconsistencyofthemixtureswas measuredwithaVe–Betestat10,20and30minaftercasting. Thefreshdensityofthemixtureswasalsorecorded.
2.2. Mechanicalanddurabilitytests
The 100mm×100mm cubic specimens were prepared for thecompressivestrengthtests.Thesetestswereconducted usingacompressivestrengthtestingmachinewithaloading rateof0.3MPa/s.Flexuralstrengthtestswereconductedon 100mm×100mm×500mmrectangularsamples.Auniversal testmachine withaloadingrate of1.00MPa/minwas also used.Thestaticmodulusofelasticityvalueswasmeasured onthedifferentmixtures(150mm×300mmcylindrical sam-ples)at90daysaccordingtotherequirementsofASTMC469 [35].Youngmodulusofelasticityvalueswasdeterminedwith thefollowingformulapresentedinEq.(1),where‘E’represents Youngmodulusofelasticity;‘1’and‘2’definecompressive
strengthwith50microstrainandstressunder40%ultimate load,respectively;and‘2’representsthelongitudinalstrain
under2stress.
E= (1−2)/(2−0.000050). (1)
Modulusofelasticitytestswereperformedonthree sam-ples from each mix. Modulus of elasticity was evaluated utilisingthe chord method. All mechanicaltests were per-formed with the guide ofEN 12390-2, EN 12390-3 and EN 13390-5standardrequirements[36–38].
ThewaterabsorptionratesoftheRCCsampleswere mea-suredaccording totheASTM C642 [39]requirements.The specimenswerefirstlydriedinanovenat105◦Cforoneday and cooled under laboratorytemperature (23◦C), and their weightswererecordedas‘W1’.Thesamesampleswereboiled
for5hinacontainerandcooledandthenboiledagain.The cooledweightswererecordedas‘W2’.Thewaterabsorption
(Wa,%)oftheRCCmixeswasdeterminedbyEq.(2).
Wa=[(W2−W1)/W1]×100. (2)
The freeze and thaw resistance of the specimens was determinedaccordingtotheASTMC666standard[40].The compressive strength losses wererecorded at90 days.The magnesium sulphateeffectontheRCCsampleswas inves-tigatedwiththecompressivestrengthchange.Onegroupwas keptincuringwater,andthesecondgroupwasexposedtothe magnesiumsulphateconcentrationsof10inaseparate con-tainer.Themagnesiumsulphateconcentrationwasrenewed every15daysuntiltheendoftestingtime(90days).The abra-sionresistanceoftheRCCmixtureswasdeterminedaccording totheASTMC418:AbrasionResistanceofConcreteby Sand-blastingstandard.
3.
Results
and
discussions
3.1. FreshandmechanicalpropertiesofRCCmixtures
As shown in Table 3, high optimum water contents were gainedwiththeincreaseinthesupplementarycementitious materialamount.Thisphenomenoncanbeattributedtothe higherspecificsurfaceareaandthesmallerspecificgravityof GCCcomparedwiththoseofcement[41].
TheconsistencyoftheRCCmixtureswasinvestigatedwith modifiedVe–Betestsat10,20and30minfollowingthe cast-ingprocessaccordingtotheASTMC1170standard[42].The Ve–BetestresultsaregiveninFig.3.TheresultsshowthatGCC addedconcretemixturesshowlessVe–Betimethanthe refer-encemixture.Withtheadditionof%5GCCtothesample,vebe timeof30mintestincreasedtwiceastheothertestresults.Itis determinedthatadditionofGCChasgreaterimpacton10min Ve-betestresultsthan20minVebetestresults.The consis-tencyofthemixturesconsiderablyimprovedascementwas replacedwithGCC.Thisimprovementcouldbeattributedto thehighfinenessvalueandpartlyroundedsurfacesoftheGCC particles(Fig.2).Thetestresultsshowedparallelresultswith thesupplementarycementmaterial-addedRCCpavement lit-erature[8,18].
The test results of wet density are presented in Fig. 4. Asshowninthefigure,GCCadditionconsiderablyincreased the wetdensity ofthe mixturescomparedwiththatofthe
Fig.4–WetdensityoftheRCCmixtures.
referencemix.Thiscondition canbeclarified bythe filling of voids by the GCC particles. As a result, the same vol-ume is filled with higher amount of mass. Figs. 3 and 4 also show that low Ve–Be times correspond with high wet density. Wet density test results also reflected the utilisation boundaries for different types of implementa-tions.
The compressive strength test results are presented in Fig.5,whereGCCinclusionupto15%increasedthetestresults comparedwiththoseofthereferencemixture.GCCinclusion alsocontributedtotheearlystrengthdevelopmentoftheRCC mixtures.However,the samplescontain10%and 15%GCC havealittleincreasein7dayscompressivestrength(0.6%and 0.9%).Thisfindingindicatesthattheuseofvariouscement replacementmaterialsor fibres haspositive effectson the compressivestrengthofRCC[43–45].ItwasobservedthatGCC mainlyactedascementreplacementmaterialandincreased thestrength.Theremainingmaterialfromthehydration pro-cessactedasfillermaterialduetoparticlesize.Ontheother hand,thecompressivestrengthvaluesofthemixtures con-tainingmorethan15%GCCcontentreducedatallages.This resultcan beattributedto the high GCCcontents and the dilutioneffect.Thosesampleshavemorethan15%ofGCC, havemorevoidsandhigherwater/cementratiowhichresults adecreaseincompressivestrength.RCC-15showedthebest performanceat42.71MPacomparedwiththatoftheotherRCC mixturesat90days.Allcompressivestrengthtestresultsat28 dayswereobtainedwithintherangeofACI325-10R require-ments[46].
The flexural strength test results at 7, 28 and 90 days are presentedinFig.6. All measuredflexural strengthtest resultsvaried between3.11 and 5.11MPa. Itis determined thatthetrendofcompressiveand flexuralstrength testsis alike.GCCadditionupto15%improvedtheflexuralstrength developmentatallages.Thisimprovementcanbeexplained asthe filler and accelerationeffects ofGCC on the hydra-tion process ofcementas stated insomeprevious studies [47–49].Thisoutcome alsosupportsthe deductionthatthe utilisationofcementreplacementfillingmaterialhasan
incre-mental impact on RCC compressive and flexuralstrengths [50].
Themodulusofelasticityresultswerechangedfrom32.17 and37.56GPa.Thereplacementofcementwith20%GCC rep-resentsasimilarmodulusofelasticityof35.04GPacompared withthatofthereferencemixture(35.20GPa).GCCinclusion up to 15% increasedthe modulusofelasticity test results. The maximum test result was obtained as 37.56GPa with the ‘RCC-15’mixture.GCCaddition intothemixturesmore than15%hadnegativeimpactontheresults.Previousreports mentionedthatGCCcouldenhancemechanicalpropertiesby providingadditionalintegratedmicrostructures[48].
3.2. DurabilitypropertiesofRCCmixtures
Waterabsorptiontestresultsat7,28and90daysarepresented inFig.7.Thewaterabsorptionratesofthespecimensvary between2.41%and3.01%at28days,andRCC-15hadthe min-imumtestresults.Unlikefibre-addedRCC[44],GCCaddition decreasedthewaterabsorptionrates.Thisdecreasecanbe attributedtothefillingoutofporesbytheGCCminerals.
The compressive strength reduction percentage of RCC mixturesareplottedinFig.8,following300freeze–thawcycles. Comparedwiththereferencemixture,compressivestrength lossesdecreasedastheGCCreplacementincreasedupto15%, andsimilarlossvalueswereobtainedfortheotherRCC mix-tures.InadditiontothepositiveeffectsofGCCadditionsonthe microstructure,theseresultscanbeattributedtotwofactors. Thedecreaseinthecompressivestrengthafterfreeze–thaw cycles issimilar tothatofanotherstudy [44],inwhichthe macro syntheticfibre-added RCCisinvestigated. The com-pressivestrengthlossescoulddecreasewiththecompactivity leveloftheRCCmixtures.AsshowninTable3,RCC-5, RCC-10andRCC-15hadbettercompaction ratioscomparedwith thoseofRCC-20andRCC-25mixtures.Itcanbeconcludedthat RCCsampleshavereachedtheoptimummixturedesignwith 15%GCCaddition.BeyondthispointGCCadditionwillrequire additionalwatertobondwiththeconcrete.Thecompressive strengthlossescanalsobeattributedtotheW/C+GCCratio.
Fig.5–Compressivestrengthtestresults.
Fig.6–Flexuralstrengthtestresults.
Theincreaseinthisratioalsoraisedthevolumeandnumber ofcapillarypores withfreezablewaterpotentialincement paste.Thesamplethathavehigherthan15%GCCaddition showhighercompressivestrengthloseafterfreezeandthaw cycles.Thistypeofeffectisexpectedasthosesampleshave morewater content and voids than the other samples. In addition,themaincauseofinternalexpansionduring freez-ing can be due to this increase as stated in the literature [41].
Theabrasion resistancetest results ofspecimens at90 daysarepresentedinFig.9.SandsconformingwiththeASTM C778[51]standardwereblastedwithaninjectortypegunat arateof690kPathroughthecentreofthespecimens.Fig.9
shows that GCC addition up to15% decreased the weight losses ofspecimens exposed duringsandblasting. Thetest results were in parallel with the mechanical compressive strength testresults.Thestrengthofmixturesisan impor-tant factorintheabrasionresistancetestresults,asstated inthe literature[43]. AllGCC hassomesilica content,and this materialpresents concerns on theabrasion resistance dependingonitsparticlesizeandconcentration[52].Notably, the utilisedBetocarb® had aconsiderableamount ofsilica content based on the improvement in abrasion resistance characteristics ofspecimenscomparedwiththatofthe ref-erencemixture.
Fig.7–Waterabsorptiontestresults.
Fig.8–Compressivestrengthlossesafterfreeze–thawcycles.
MagnesiumsulphateresistanceofRCCmixturesis plot-tedinFig.10.RCC-5,RCC-10andRCC-15specimensshowed the lowest compressive strength losses compared with the other mixtures. The overall test results indicated that cement replacement with certain amounts of GCC (up to 15%)had asignificant effect onRCC interms ofdurability properties. Utilisingcertain amounts ofGCC enhancedthe sulphateresistancebehavioursoftheRCC mixturesby fill-ingvoidsinitsstructures.Theeffectsofmagnesiumsulphate attacksalsoincreasedwiththe exposuretimeasshown in Fig.10.
Figs.11and 12representtheSEMimagesoftheRCC-15 specimenswithmagnificationsof1000×and5000×, respec-tively. Thefigures show thatthe pores are filled withGCC particles. This phenomenon can be attributed to reduced waterabsorptionrateandimprovedtransportationproperties ofthespecimen.
Fig.12showsthatporesarequitereplacedwiththeGCC particles.BycomparingFigs.11and12,thecompletefillingof poresinthescannedareaswasalsoobserved.
4.
Conclusion
The influences of utilising GCC as cement supplementary materials on the RCC mixtures were examined in this research.Themainconclusionofthisstudycanbedrawnas follows.
• CementreplacementwithGCCupto15%increasedthe opti-mumwatercontentofthemixturescomparedwiththatof thereference.
• UtilisingGCCupto15%alsoresultedinlowwater absorp-tion rates and less compressive strength losses against
Fig.9–Weightlossesofspecimensexposedtosandblasting.
Fig.10–Compressivestrengthlossesaftermagnesiumsulphateattack.
freeze–thawcycles.Thiscanbeattributedtofillerand poz-zolaniceffectofGCC.WiththeadditionofGCCresultsin decreaseinvoidsofthespecimens.
• The early strength characteristics of specimens were enhancedwithacertainamountofGCCinclusionthatis resultofthepositiveeffectofGCCadditioninthehydration processofcement[25].
• Magnesium sulphate attacked the resistance ofthe RCC improvedwiththepreparedmixtures.RCC-15showedthe bestperformanceagainstsulphateattacks.Duetoreduce intheporewiththeadditionofGCC,theeffectofsulphate attacksdecreases.
• Atotalof15% cementreplacementwithGCCwasfound tobeeffectivethroughstrengthanddurabilityproperties. Thisapproachcanbeutilisedforcostoptimisationstudies ofRCCmixtures.
• Similartoutilisationofflyash[50],GCCincorporationalso has a positive impact in reducing the pores in RCC as observedintheSEManalysisfigures.
• Besidesimprovingmechanicalanddurabilitypropertiesof concrete,GCCadditionmightbebeneficialtoproduce sus-tainableconcrete.WiththeuseofGCCascementreplacing material,lessenergyconsumedduringcementproduction. InthisrespectlessCO2willbereleasedfromthefactories.
Fig.11– SEMimagesoftheRCC-15specimenat1000×magnification.
Fig.12– SEMimagesoftheRCC-15specimenat5000×magnification.
Conflicts
of
interest
Theauthorsdeclarenoconflictsofinterest.
Acknowledges
Theauthorswouldliketoacknowledgetothestaffof KMU-BILTEMfortheirhelpandsupports.
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